DOI: https://doi.org/10.55373/mjchem.v26i3.161

Keywords: 2D Materials; MAX phase; V2AlC MAX phase; Ball milling; Sustainability

Abstract

In this study, we present a comprehensive optimization study for the synthesis of the V2AlC MAX phase by systematically investigating the effects of key parameters, including precursor ratios, reaction temperature, reaction time, and heating rate. The resulting V2AlC MAX phase samples are characterized using X-ray diffraction, scanning electron microscopy, and energy dispersive X-ray spectroscopy analysis to evaluate their phase purity, structure, and morphological features. The optimum temperature for the synthesis of V2AlC MAX phase is 1500°C with a holding time of 4 h at a heating rate of 5°C to achieve MAX phase with a high quality. The optimized synthesis conditions outlined in this study serve as a fundamental basis for scaling up the yield of the V2AlC MAX phase in a more sustainable and efficient approach and subsequently enable the wider adoption of V2AlC MAX phase in various applications, promoting a sustainable future.