MALAYSIAN JOURNAL OF CHEMISTRY (MJChem)

MJChem is double-blind peer reviewed journal published by the Malaysian Institute of Chemistry (Institut Kimia Malaysia) E-ISSN: 2550-1658

The Physicochemical and Electrochemical Characterization of Silver Nanoparticle-Incorporated Magnetite/Reduced Graphene Oxide

Azleen Rashidah Mohd Rosli
Universiti Malaysia Terengganu
Nur Ayunie Kamaruzaman
Universiti Malaysia Terengganu
Ainul Mardhiah Mansor
Universiti Malaysia Terengganu
Wan M. Khairul
Universiti Malaysia Terengganu
Farhanini Yusoff
Universiti Malaysia Terengganu
Noorashikin Md Saleh
Universiti Kebangsaan Malaysia

DOI: https://doi.org/10.55373/mjchem.v25i4.73

Keywords: Electrocatalyst; silver nanoparticles; magnetite; reduced graphene oxide

Abstract

In this paper, the physicochemical characterization and electrochemical behavior of a newly developed silver nanoparticle-incorporated magnetite/reduced graphene oxide (Ag-Fe3O4/rGO) are presented. The composites were synthesized by a simple approach of synthesis route combining the Hummer’s method for synthesis of graphene oxide and the co-precipitation method for preparation of iron oxide. The physical characterization of the composites was studied using Fourier Transform Infrared (FTIR) spectroscopy, X-Ray Diffraction (XRD) analysis, Scanning Electron Microscopy (SEM), and Brunaeur-Emmet-Teller (BET) technique. Cyclic voltammetry (CV) technique and Electron Impedance Spectroscopy (EIS) were employed to study the electrochemical properties of Ag-Fe3O4/rGO. Results from the analyses signify a good electron transfer characteristic with high conductive and excellent capacitor nature of the modified electrocatalyst.

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Published 24 September 2023


Issue Vol 25 No 4 (2023): Malaysian Journal of Chemistry

Section